Materials Literature
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Zero valent Cu polyamidoamine (PAMAM) dendrimer nanocomposites were synthesized using UV irradiation starting from the aqueous Cu(II)/dendrimer system. The size of the nanoparticles is strongly dependent on the generation of the dendrimers and the pH of the solution. Larger nanoparticles are obtained with higher gener…
Natural cellulose fibres have been employed for packaging applications for a long time. Their use, however, has been hampered by their high hydrophilicity and their moisture sensitivity. It has, thus, been proposed to circumvent this problem through the hydrophobic modification of their surface thanks to the use of mo…
Photoluminescence (PL) and optically detected magnetic resonance are employed to study effects of nonstoichiometry during the growth on defect formation in ZnO epilayers grown by molecular-beam epitaxy (MBE). Several defects are revealed via monitoring the yellow PL emission (∼2.17eV) and their magnetic resonance sign…
We investigated the blue luminescent silicon nanocrystal (Si-nc) preparation in liquid spin on glass (SOG) by nanosecond laser ablation of the Si target in SOG. The confinement of laser-generated plasma in liquids significantly enhanced the formation of Si-nc. Furthermore, the silicon-dioxide-based SOG inhibited Si-nc…
Magnetization measurements as a function of temperature and magnetic field were performed on polyimide nanocomposite samples containing various weight percentages of single wall carbon nanotubes. It was found that the magnetization of the composite, normalized to the mass of nanotube material in the sample, decreased…
We experimentally studied a nematic liquid crystal whose molecules form twisted head-to-head H-bonded dimers. We observed that when the material transformed from the isotropic to nematic phase, it formed droplets with chiral propeller textures. We carried out a computer simulation to investigate the liquid crystal dir…
Abstract The benzylation of benzene and substituted benzenes reaction employing benzyl chloride as the alkylating agent over Mg‐Fe‐LDH (Mg/Fe = 2) clay without or with calcination (at 473–1073 K) has been investigated. Hydrotalcite before and after its calcination was characterized for surface area and crystalline pha…
Regular arrays of Si nanorods with a circular cross section in hexagonal-closed-packed and triangular cross section in honeycomblike arrangements were grown using glancing angle deposition on Si(100) and fused silica substrates that were patterned with Au dots using self-assembled mono- and double layers of polystyren…
We have investigated the crystallization of amorphous equiatomic NiTi thin films sandwiched between two protective silicon nitride barrier films using optical, atomic force, and transmission electron microscopies. Crystallite nucleation occurs homogeneously inside the NiTi films because small composition shifts at the…
Potentiostatic intermittent titration technique (PITT) and electrochemical impedance spectroscopy (EIS) were investigated as methods to determine solid phase chemical diffusion coefficient (D) and electronic density of states (DOS). These techniques were then applied to iridium oxide (IrOx) and iridium-tantalum oxide…
A series of Ni(1−x)FexO (x=0, 0.015, 0.03, 0.05, and 0.1) bulk samples was synthesized by the chemical concentration-precipitation method. Phase composition analysis was carried out, which showed that trace amounts of ferromagnetic phase NiFe2O4 could not be detected by x-ray diffraction in these bulk samples with x≤0…
The Co-doped ZnO thin films were prepared on c-cut sapphire substrates by magnetron cosputtering, and then annealed at various temperatures in vacuum. Magnetic measurements indicate that all the films are ferromagnetic at room temperature and the magnetization of the annealed Zn0.88Co0.12O films is increased about one…
Maxwell relation and mean-field approximation are chosen to estimate the total entropy change and the magnetic entropy change, respectively. The experimental results are exactly consonant with the theoretical results. Consequently, the magnetic entropy changes make up the majority of the total entropy change, and the…
The origin of size effects in the thermal conductivity and diffusivity of nanostructural semiconductors was investigated through the establishment of a unified nanothermodynamic model. The contributions of size-dependent heat capacity and cohesive energy as well as the interface scattering effects were considered duri…
The magnetocaloric effect (MCE) has been observed in three well-defined temperature intervals (region I: 2–115 K, region II: around charge order transition TCO, and region III: around room temperature) in polycrystalline Nd0.5Ca0.5MnO3 (NCMO) manganite system showing a first order (CO) transition at a temperature, TCO…
The surface of a biomaterial interacts with the body fluid upon implantation in the human body. The biocompatibility of a material is strongly influenced by the adsorption of proteins onto the surface. Titanium is frequently used as a biomaterial for implants in orthopedics and cardiovascular devices. Understanding th…
Resonant Raman spectroscopy studies of (Mn, Co)-codoped ZnO films were carried out using the 325 nm laser as the excitation source. The mixed mode character of the longitudinal optical (LO) phonon reveals that the resonant Raman spectra of the films can be used to test the c-axis orientation degree of their crystallit…
Molecular dynamics results for the dynamic Prigogine-Defay ratio are presented for two glass-forming liquids, thus evaluating the experimentally relevant quantity for testing whether metastable-equilibrium liquid dynamics is described by a single parameter to a good approximation. For the Kob-Andersen binary Lennard-J…
The pressure as a function of volume and temperature has been investigated for B2-type NaCl over the pressure range of 20–360GPa and at temperatures between 300 and 3000K. The simulations were performed using ab initio molecular dynamics method within the density-functional theory framework. A Vinet equation of state…
The heterostructure and compositional depth profile of low-temperature processed (Pb 0.76 Ca 0.24 )TiO 3 (PCT24) ferroelectric thin films have been studied in the present work. The films were prepared by ultraviolet (UV) sol–gel photoannealing (also called photochemical solution deposition, PCSD) onto platinized silic…