Materials Literature
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The fracture strength of ZnO nanowires vertically grown on sapphire substrates was measured in tensile and bending experiments. Nanowires with diameters between 60 and 310 nm and a typical length of 2 µm were manipulated with an atomic force microscopy tip mounted on a nanomanipulator inside a scanning electron micros…
The rare-earth ions (RE = Eu, Dy Ho, Tm, Y) doped charge-ordered antiferromagnetic manganites, Pr 0.45 RE 0.05 Ca 0.5 MnO 3 , were studied for the magnetic and the transport properties in the presence of external magnetic fields of up to 14 tesla. Regardless of the intrinsic magnetic property of RE ions, all the compo…
First principles calculations were performed to study the ground state electronic properties of BaFeO3 (BFO) within the density functional theory (DFT). Adopting generalized gradient approximation (GGA) exchange and correlation functional and Vosko-Wilk-Nusair correlation energy functional interpolation, we have syste…
The authors present the structure transformation and magnetic properties of Bi1−xLaxFeO3 (x=0.0–0.15) ceramics prepared by a conventional solid-state reaction processing. Magnetic measurements reveal that remnant magnetization of 15% La-doped BiFeO3 has enhanced about 20 times as compared to pure BiFeO3. It is the str…
Regularly twinned domain structures are observed by scanning piezoforce microscopy on single crystalline grains of BiFeO3 ceramics being grown by a special low temperature sintering process. The domains are considerably larger than those observed in thin films. Their spontaneous polarization comes close to that predic…
Dropwise condensation can enhance heat transfer by an order of magnitude compared to film condensation. Superhydrophobicity appears ideal to promote continued dropwise condensation which requires rapid removal of condensate drops; however, such promotion has not been reported on engineered surfaces. This letter report…
Monte Carlo simulations have been widely used by microscopists for the last few decades. In the beginning it was a tedious and slow process, requiring a high level of computer skills from users and long computational times. Recent progress in the microelectronics industry now provides researchers with affordable deskt…
The long-ranged elastic model, which is believed to describe the evolution of a self-affine rough crack-front, is analyzed to linear and non-linear orders. It is shown that the nonlinear terms, while important in changing the front dynamics, are not changing the scaling exponent which characterizes the roughness of th…
We report the observation of a compensation point in the temperature dependence of magnetization data of polycrystalline Sm2Al. Magnetization measurements show that this compound magnetically orders at about 150 K. Below this temperature, the magnetization data shows a compensation point, which shifts with field. Hyst…
Abstract PS@CdS core–shell nanostructures were fabricated by microwave irradiation at 70 °C from the aqueous solution of CdCl2, TAA, and PVP with PS microspheres without surface modification. The products were investigated by XRD, FE-SEM, TEM, IR, and Raman. CdS hollow spheres were easily obtained by removing the PS c…
Abstract Silver dendritic hierarchical structures have been prepared using a simple, surfactant-free method by carrying out the silver mirror reaction on the surface of a porous anodic aluminium oxide (AAO) template. The surface of the AAO template has a guiding effect in the formation process of silver dendritic hier…
In this work, high-energy ball-milled magnesium hydride samples used for hydrogen storage are investigated using small- and ultra-small-angle neutron scattering (SANS) as well as small-angle X-ray scattering (SAXS). Size distributions of inhomogeneities with dimensions from 10 Å up to more than 10 µm, corresponding to…
A novel facile method has been demonstrated for large-scale synthesis of zinc-oxide-based one-dimensional solid solution with a series percentage of nickel dopant. The obtained Zn1-xNixO nanorods were characterized by X-ray diffraction, transmission electron microscopy, selected area electron diffraction, and energy d…
Infrared reflection absorption spectroscopy and X-ray reflectivity have been used to elucidate the molecular orientation and hydrocarbon chain conformation and packing of the symmetric long-chain bolaamphiphiles dotriacontane-1,1'-diyl-bis-[2-(trimethylammonio)ethylphosphate] (PC-C32-PC) and dotriacontane-1,1'-diyl-bi…
This study investigates the adsorption and reactions of boron trichloride and its fragments (BClx) on the TiO2 anatase (101) and rutile (110) surfaces by first-principles calculations. The results show that the possible absorbates on the TiO2 anatase and rutile surfaces are very similar. The single- and double-site ad…
Crystal cryocooling is usually employed to reduce radiation damage during X-ray crystallography. Recently, a high-pressure cryocooling method has been developed which results in excellent diffraction-quality crystals without the use of penetrative cryoprotectants. Three new developments of the method are presented her…
The hierarchical structure of an aqueous dispersion of niobate nanosheets was explored by using a combined method of ultra-small-angle and small-angle scattering of neutrons and X-rays. The concentration of the sheets studied was in the range where the dispersion exhibits a liquid-crystal phase as evidenced by observa…
The molecular structure of the chloro-dodecafluorosubphthalocyaninato boron(III) (F-SubPc) was determined with use of Gas Electron Diffraction (GED) and high-level quantum chemical calculations. The present results show that the F-SubPc molecule has a cone-shaped configuration, isoindole units are not planar, and the…
We have developed a simple wet-chemistry approach to fabricating ZnO submicrometer particles with unique morphologies including rings, bowls, hemispheres, and disks. The size and morphology of the particles can be conveniently tailored by varying the concentrations of the zinc precursor. The reaction temperature, pH,…
The facile solid-solid phase transformation of TCNQ microcrystals into semiconducting and magnetic Ni[TCNQ]2(H2O)2 nanowire (flowerlike) architectures is achieved by reduction of TCNQ-modified electrodes in the presence of Ni2+(aq)-containing electrolytes. Voltammetric probing revealed that the chemically reversible T…