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Refinement of the crystal structure of arsenolite, AS2O3

Paolo Ballirano、Adriana Maras2002-12-01Zeitschrift für Kristallographie - New Crystal Structures

As2O3, cubic, Fd (3) over barm (No. 227), a = 11.07343(5) Angstrom, V = 1357.8 Angstrom(3), Z = 16, R(P) = 0.056, wR(P) = 0.073, R(I) = 0.068, T = 295 K.

High-pressure geophysics and materialsCrystal Structures and PropertiesX-ray Diffraction in Crystallography

Detailed Structural Characterizations of SBA‐15 and MCM‐41 Mesoporous Silicas on a High‐Resolution Transmission Electron Microscope

Hong‐Ping Lin、Chih‐Yuan Tang、Ching‐Yen Lin2002-12-01Journal of the Chinese Chemical Society

Abstract Using high‐resolution transmission electronic micrograph (HR‐TEM) observation, one can clearly see the pore geometry of the MCM‐41 and SBA‐15 mesoporous silicas to determine that their pore shapes are hexagonal and round, respectively. With the perpendicular orientations of the nanochannels to the electron be…

Catalytic Processes in Materials ScienceZeolite Catalysis and SynthesisMesoporous Materials and Catalysis

Synergistic inhibition of carbon steel corrosion by sodium tungstate and sodium silicate in neutral aqueous media

Viswanathan S. Saji、S.M.A. Shibli2002-12-01Anti-Corrosion Methods and Materials

Tungstate inhibitors are seldom used alone in open recirculating cooling water systems due to their low oxidising ability and high cost. The objective of the present work was to develop efficient synergistic inhibitor combinations comprising sodium silicate and very low concentration of sodium tungstate, keeping in vi…

Corrosion Behavior and InhibitionConcrete Corrosion and DurabilityMagnesium Oxide Properties and Applications

Solid Solubility and Precipitation in a Single‐Crystal Alumina–Zirconia System

Matthew A. Stough、John R. Hellmann2002-12-01Journal of the American Ceramic Society

Solid solubility was examined in Zr‐doped sapphire and Al‐doped yttria‐stabilized zirconia (YSZ) single crystals from 1200° to 1600°C. Specimens were fabricated via ion implantation of single crystals, followed by annealing in air. Secondary ion mass spectroscopy (SIMS) was used to quantify solute redistribution durin…

Advanced ceramic materials synthesisGlass properties and applicationsNuclear materials and radiation effects

Iron (II) Phosphate (Fe3(PO4)2 by XPS

Yuqing Wang、Daniel J. Asunskis、Peter M. A. Sherwood2002-12-01Surface Science Spectra

The XPS spectra of ferrous phosphate were collected with a VSW HA150 using monochromatic Al Kα x-radiation. Monochromatic radiation provides a distinct clarity to the rich peak structure in the valence band of ferrous phosphate due to the absence of interfering x-ray satellites from the intense O 2s region. The valenc…

Electron and X-Ray Spectroscopy TechniquesChemical Synthesis and CharacterizationX-ray Diffraction in Crystallography

The Characterization of a New Pale Blue Corrosion Product Found on Copper Alloy Artifacts

Karen Trentelman、Leon P. Stodulski、David Scott 等 11 位作者2002-12-01Studies in Conservation

A new pale blue corrosion product has been found on copper alloy artifacts in the collections of a number of institutions. The corrosion product has been characterized using X-ray powder diffraction, X-ray photoelectron spectroscopy, wavelength X-ray dispersive spectroscopy and Raman microspectroscopy. The corrosion p…

Corrosion Behavior and InhibitionCultural Heritage Materials AnalysisElectron and X-Ray Spectroscopy Techniques

Ability of some Norwegian soils to supply grass with potassium (K) ‐ soil analyses as predictors of K supply from soil

Anne Falk Øgaard、Tore Krogstad、Tor Lunnan2002-12-01Soil Use and Management

Abstract. Uptake in grass crops of ammonium acetate lactate extractable K (K AL ) and reserve K (interlayer K + structural K) in soil was studied in 16 field experiments at different locations on a range of mineral soil types in Norway. The K uptake from soil, both from K AL and reserve K, was considerable, often even…

Soil Carbon and Nitrogen DynamicsSoil and Unsaturated FlowClay minerals and soil interactions

Electrical insulation characteristics of cold dielectric high temperature superconducting cable

H. Suzuki、T. Takahashi、Tatsuki Okamoto 等 5 位作者2002-12-01IEEE Transactions on Dielectrics and Electrical Insulation

For the optimization of electrical insulation design for high temperature superconducting (HTS) cable, evaluation of electrical insulation characteristics especially for butt gap of LN/sub 2/ impregnated cold dielectric (CD) which consists of the wrapped tape insulation impregnated with LN/sub 2/ plays an important ro…

High voltage insulation and dielectric phenomenaHVDC Systems and Fault ProtectionSuperconducting Materials and Applications

Analysis of membrane stereochemistry with homology modeling of sn-glycerol-1-phosphate dehydrogenase

Hiromi Daiyasu、Takaaki Hiroike、Yosuke Koga 等 4 位作者2002-12-01Protein Engineering Design and Selection

Different enantiomeric isomers, sn-glycerol-1-phosphate and sn-glycerol-3-phosphate, are used as the glycerophosphate backbones of phospholipids in the cellular membranes of Archaea and the remaining two kingdoms, respectively. In Archaea, sn-glycerol-1-phosphate dehydrogenase is involved in the generation of sn-glyce…

Genomics and Phylogenetic StudiesEnzyme Catalysis and ImmobilizationEnzyme Structure and Function

Quantitative analysis of mineralized white Portland clinkers: The structure of Fluorellestadite

I Pajares、Ángeles G. De la Torre、S. Martínez‐Ramirez 等 6 位作者2002-12-01Powder Diffraction

Fluorellestadite, Ca 10 (SiO 4 ) 3 (SO 4 ) 3 F 2 , has been synthesized as single phase. This compound crystallizes in the apatite type structure, s.g. P6 3 /m, with parameters a =9.4417(1) Å, c =6.9396(1) Å and V =535.76(1) Å 3 . The refinement of its crystal structure converged to R WP =12.33% and R F =4.58%. The at…

Advanced ceramic materials synthesisNuclear materials and radiation effectsX-ray Diffraction in Crystallography

Fabrication of Flexible Distributed Feedback Laser Using Photoinduced Surface Relief Grating on Azo-Polymer Film as a Template

Tatsunosuke Matsui、Masanori Ozaki、Katsumi Yoshino 等 4 位作者2002-12-01Japanese Journal of Applied Physics

An all-polymer flexible distributed feedback (DFB) laser has been fabricated using a photoinduced surface relief grating (SRG) on an azo-polymer film as a template. The holographically induced SRG on the azo-polymer was transferred onto a flexible film of a UV-curable photopolymer. Optically pumped mirrorless DFB lase…

Photonic and Optical DevicesLiquid Crystal Research AdvancementsNonlinear Optical Materials Studies

Molecular Dynamics Study of Hypothetical Silicon Nanotubes Using the Tersoff Potential

Jeong Won Kang、Jae Jeong Seo、Sung‐Ho Hwang2002-12-01Journal of Nanoscience and Nanotechnology

We have performed classical molecular dynamics simulations for hypothetical silicon nanotubes using the Tersoff potential. Our investigation presented a systematic study about the thermal behavior of hypothetical silicon nanotubes and showed the difficulty in producing silicon nanotubes or graphitelike sheets. However…

Carbon Nanotubes in CompositesGraphene research and applicationsBoron and Carbon Nanomaterials Research

Aluminum Nitride Prepared by Nitridation of Aluminum Oxide Precursors

Edwin Kroke、Lars Loeffler、Fred F. Lange 等 4 位作者2002-12-01Journal of the American Ceramic Society

Aluminum nitride (AlN) powders were prepared from the oxide precursors aluminum nitrate, aluminum hydroxide, aluminum 2‐ethyl‐hexanoate, and aluminum isopropoxide (i.e., Al(NO 3 ) 3 , Al(OH) 3 , Al(OH)(O 2 CCH(C 2 H 5 )(C 4 H 9 )) 2 , and Al(OCH(CH 3 ) 2 ) 3 ). Pyrolyses were performed in flowing dry NH 3 and N 2 at 1…

GaN-based semiconductor devices and materialsAdvanced ceramic materials synthesisSemiconductor materials and devices

A Systematical Method for Suppressing Ferroresonance at Neutral-Grounded Substations

Yunge Li、Rui Qin、Junqiang Yang 等 4 位作者2002-12-01IEEE Power Engineering Review

At neutral-grounded substations, ferroresonance may happen upon switching a circuit breaker or disconnector due to the saturated magnetizing characteristics of the bus PT. A systematical method is presented to analyze and suppress the phenomenon. The scheme for suppressing the ferroresonance is to insert resistance, m…

Magnetic Properties and ApplicationsPower Systems and TechnologiesGeoscience and Mining Technology

Effects of temperature and strain rate on the tensile behavior of unfilled and talc‐filled polypropylene. Part II: Constitutive equation

Yuanxin Zhou、P. K. Mallick2002-12-01Polymer Engineering and Science

Abstract Based on the experimental results presented in Part I of this research, a three parameter nonlinear constitutive model has been proposed to describe the strain rate and temperature dependent tensile behaviors of unfilled and talc‐filled polypropylene. One of the parameters is the elastic modulus. The other tw…

Mechanical Behavior of CompositesPolymer crystallization and propertiesPolymer Nanocomposites and Properties

Magnetic phase diagram of the Bi1-x CaxMnO3 manganites

I. O. Troyanchuk、O. S. Mantytskaya、A. N. Chobot2002-12-01Physics of the Solid State

The magnetic and elastic properties of the Bi1-x CaxMnO3 manganites are studied. The phase transformations revealed are ferromagnet-spin glass (x≥0.15) and spin glass-charge-ordered antiferromagnet (x≥0.25). The ferromagnetic state is characterized by ordering of the Mn3+ d x 2-y orbitals. It is suggested that thespin…

Magnetic and transport properties of perovskites and related materialsShape Memory Alloy TransformationsMultiferroics and related materials

Spectroimmunochemistry Using Colloidal Gold Bioconjugates

Alexander A. Kamnev、Lev A. Dykman、Petros Α. Tarantilis 等 4 位作者2002-12-01Bioscience Reports

Using surface-enhanced infrared absorption (SEIRA) spectroscopy of dry films of colloidal gold (CG) bioconjugates with protein A, it is shown that certain characteristic bands of the protein (e.g., amide I, amide II and some other vibration modes) are essentially affected by the metal surface. Thus, the method may be…

Gold and Silver Nanoparticles Synthesis and ApplicationsSpectroscopy Techniques in Biomedical and Chemical ResearchElectrochemical Analysis and Applications

Raw Materials for Low-Activation Concrete Neutron Shields

Masaharu Kinno、Ken‐ichi Kimura、T. Nakamura2002-12-01Journal of Nuclear Science and Technology

Concrete surrounding a nuclear reactor accumulates radioisotopes induced by neutron reactions during operation, and this concrete still remains to an enormous degree as radioactive waste after decommissioning. The disposal of such activated concrete is very costly and requires strict supervision. Hence, there has been…

Nuclear reactor physics and engineeringGraphite, nuclear technology, radiation studiesNuclear and radioactivity studies

Gadolinium-Ethoxybenzyl-Diethylenetriamine-Pentaacetic Acid Interaction With Clinical Drugs in Rats

Naoki Kato、Takashi Yokawa、Ayako Tamura 等 6 位作者2002-12-01Investigative Radiology

RATIONALE AND OBJECTIVES: To investigate whether the hepatic enhancement characteristics of Gd-EOB-DTPA are influenced by the preapplication of a variety of commonly used clinical pharmaceuticals (eg, antibiotics, antineoplastic drugs, corticosteroids, antiarrhythmia drugs, antianxiety drugs, scopolamine, and xanthine…

Drug Transport and Resistance MechanismsLanthanide and Transition Metal ComplexesChemotherapy-induced organ toxicity mitigation

AGE RELATED CHANGES IN POULTRY BREAST MEAT COLLAGEN PYRIDINOLINE AND TEXTURE

Fábio Augusto Garcia Coró、Elza Youssef Youssef、Massami Shimokomaki2002-12-01Journal of Food Biochemistry

Pyridwotine (PYR), a mature collagen crosslink, -was measured in Ross hen breast meat, Pectoralis major, age ranging from 20 to 540 days and its concentration varied between 0.009 to 0.101 mol/mol collagen, respectively. PYR concentration was inversely related to collagen solubility in muscle homogenates (P>0.05) and…

Meat and Animal Product QualityCollagen: Extraction and Characterization