Materials Literature
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Cobalt(II) phthalocyanine (CoPc), cobalt(II) tetrachloro phthalocyanine (CoPcCl4), cobalt(II) octachloro phthalocyanine (CoPcCl8) and cobalt(II) hexadecachloro phthalocyanine (CoPcCl16) are synthesized pure and characterized using elemental analysis, UV-visible, IR-spectroscopy, magnetic susceptibility, X-ray crystall…
The catalytic partial oxidation of methane to syngas presents interesting challenges, because of the interaction of exothermic combustion and endothermic reforming reactions. The heterogeneous plug-flow and axial-dispersion models are used to analyze the steady-state and dynamic behavior exhibited by this process in a…
BiFeO 3 thin films were processed on La0.8Sr0.2MnO3 (LSMO) buffered silicon substrate via chemical solution deposition. Short-wave ultraviolet assisted pyrolysis was conducted in oxygen atmosphere in order to improve microstructure. A fine, homogeneous, and phase-pure grain structure with smooth topography was obtaine…
Field emission properties of a stand-alone MgO-coated carbon nanotube (CNT) have been investigated by a field emission microscopy. A finite element method is used to analyze the electric field distribution on the surface of a CNT and in the layer of MgO. It is found that the dielectric MgO layer decreases the strength…
Complicated domain configurations generated during the magnetization reversal of Permalloy elements patterned in various shapes are the results of a surprisingly few switching mechanisms. By comparing the results from micromagnetic simulations with the experimentally observed switching events imaged by Lorentz microsc…
We combine the self-assembly properties of amphiphilic molecules with the radiolysis method to produce specific sizes and shapes of metallic nano-objects. Radiolysis is used to synthesize core--shell structures consisting of nanometric linoleate spherical micelles as the core and silver as the shell. The validity of t…
The optomechanical effect and photoinduced anisotropic deformation induced by illumination of linearly polarized light have been comparatively studied for glassy As2S3 and Se films. The two materials show qualitatively the same behaviors in the mechanical effect and the deformation, which suggests that these photoindu…
It is important to research activation of the slip systems in magnesium crystals to understand deformation behavior of magnesium. In this study, pure magnesium, Mg-7.0at%Li and Mg-0.1at%Zn single crystals were stretched in the [11-20] direction in the range of 77K to 573K to investigate the deformation behavior by non…
Using a layer-by-layer (LbL) sequential adsorption technique, we studied the construction of hydrogen-bonded multilayers of a weak polycarboxybetaine (poly- N -ω-carboxypentyl-4-vinylpyridinium bromide (PCB5)) with poly( N -vinylcaprolactam) (PVCL). Self-assembly occurred at low pH values where carboxylic groups of PC…
Recently, plasma deposited amorphous carbon films have been the subject of extensive experimental and theoretical investigations aimed at correlating their electronic, structural, and mechanical properties to growth parameters. To investigate these properties, different spectral parameters reflecting the electronic st…
Silicon nanocrystals embedded in a silicon-rich silicon-oxide matrix have been fabricated at different silicon contents (38%, 40%, and 49%) using plasma-enhanced chemical vapor deposition and annealing at different temperatures in the range from 900 °C to 1100 °C. Their optical properties have been investigated by pho…
The impact of chemical ordering on the dielectric properties of the thin film relaxor Pb(Sc1∕2Ta1∕2)O3 (PST) was investigated. It was found that the dielectric permittivity increased with increased B site order, directly opposite the behavior observed in ceramics. Highly ordered PST thin films on sapphire substrates w…
The process of nucleation of multiwall carbon nanotubes in chemical vapor deposition process with nickel as catalyst and methane as a carbon precursor is analyzed. The nucleation is considered as a specific instability developed on the surface of a metal catalyst particle supersaturated with carbon. The energy release…
Empirical tight-binding calculations on the layer compound $2H\text{\ensuremath{-}}\mathrm{Ta}{\mathrm{Se}}_{2}$ have been performed and are found to replicate the basic phenomenology of Fermi surface topology and charge-density-wave gapping as revealed by angle-resolved photoemission spectroscopy (ARPES). The recentl…
The line emissions of OH*, Na, Na-Ar*, and Ar are observed in stable and bright single bubble sonoluminescence (SBSL), which shows that the composition of the bubble consists of at least three parts: the vapor, droplets of the host liquid, and the gas dissolved in the host liquid. The observation of line emissions in…
Abstract A tris‐silylated urea‐based compound, 1,3,5‐tris(triethoxysilylpropylureido)benzene has been synthesized. Hybrids materials with different shapes (films, spheres and tubes) are obtained upon base‐catalyzed hydrolytic condensation of this compound. A self‐templating process is demonstrated using electron micro…
The local structure of Na-Al-P-O-F glasses, prepared by a novel sol-gel route, was extensively investigated by advanced solid-state NMR techniques. 27Al{19F} rotational echo double resonance (REDOR) results indicate that the F incorporated into aluminophosphate glass is preferentially bonded to octahedral Al units and…
PAMAM-Au nanocomposites prepared by reduction of HAuCl4 with NaBH4 in the presence of the sixth-generation polyamidoamine (PAMAM) took a unique structure, in which the 2 nm-sized Au nanoparticles were encapsulated in the interior cavities of the PAMAM molecules. The PAMAM-Au nanocomposites as a new type of nanomateria…
The carboxylate ligand-exchange reaction of copper(I) trifluoroacetate by 3,5-difluorobenzoate yielded a new product, [Cu(O2C(3,5-F)2C6H3)] (1). Single crystals of 1 suitable for X-ray structural characterization were obtained by sublimation-deposition procedures at 230 degrees C. An X-ray diffraction study revealed a…
Abstract Waste ground rubber tire (WGRT) is a complex composite containing various elastomers, carbon black, zinc oxide, stearic acid, processing oils, and other curatives. Most of the waste ground rubber tire is composed of mainly natural rubber (NR) and styrene butadiene rubber (SBR) in varying proportions. Blending…