Materials Literature
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Abstract Glass substrates were spin‐coated with a perfluoropolyether oligomer based organic‐inorganic hybrid material, and prepared by the sol‐gel process. Contact angle analysis and atomic force microscopic analysis were carried out to characterize the surface of the prepared coatings. All systems exhibited strong hy…
The surface of cotton fabric was successfully functionalized with vinyltrimethoxysilane in order to impart water repellency and wrinkle recovery and to introduce surface vinyl groups (—CH=CH 2 ) to the fabric, which could then be initiated for copolymerization reactions with various monomers. The introduction of activ…
Zeólita A e hidroxisodalita foram sintetizadas a partir de um rejeito industrial do processo de beneficiamento de caulim para papel, de indústrias da região amazônica. Esse rejeito é composto essencialmente por caulinita e possui razão SiO2/Al2O3 igual à requerida para esses dois tipos de zeólitas. Dessa maneira, o pr…
( 1 − x ) [ ( K 0.4725 Na 0.4725 Li 0.055 ) NbO 3 ] − x AgTaO 3 [ ( 1 − x ) KNNL − x AT ] lead-free ceramics have been prepared by the conventional mixed oxide method. Effect of the AgTaO3 (AT) content on the microstructure and electrical properties of (1−x)KNNL−xAT ceramics were systematically investigated. A morphot…
We previously reported on a decomposition system of organic wastes by the use of thermally excited holes in TiO 2 at high temperatures. A good feature of our system is that it makes use of a large number of holes formed, for example, at 350 °C for the oxidation of organic wastes. In this investigation, we aim at apply…
The ultraviolet (UV) light‐absorbing properties of the liquid crystal (LC) constituent during the photo‐induced elaboration of a cholesteric LC (CLC) gel may induce the broadening of the reflection bandwidth of the material, a situation that is promoted by asymmetrical irradiation conditions (only one side of the cell…
The influence of mechanical stimulation on cell populations not only helps maintain the specific cellular phenotype but also plays a significant role during differentiation and maturation of plastic cells. This is particularly true of tissue-engineered vascular tissue, where in vivo shear forces at the blood interface…
Determination of protein crystal structures is dependent on the growth of high-quality single crystals, a process that is not always successful. Optimum crystallization conditions must be systematically sought for, and microcrystalline powders are frequently obtained in failed attempts to grow the desired crystal. In…
Chlorophyll a and chlorophyll b exhibit distinct spectra yet differ only in the nature of a single substituent (7-methyl versus 7-formyl, respectively). Two complementary approaches have been developed for the synthesis of 7-substituted chlorins. The first approach is a de novo route wherein 2,9-dibromo-5-p-tolyldipyr…
The discovery of carbon nanotubes (CNTs) created much excitement and stimulated extensive research into the properties of nanometer-scale cylindrical networks. From then on, various methods for the synthesis and characterization of aligned CNTs-both single-walled (SWCNTs) and multi-walled (MWCNTs) by different methods…
Abstract Investment casting offers high‐quality castings with good dimensional accuracy, being therefore suitable for aircraft applications. Since commercial ceramic shells react with Mg melts and appropriate inhibitors being not available, magnesium alloys are not widely used in industrial investment‐casting. In orde…
Optical spectroscopy and volume “swelling” measurements were used to study radiation damage and graphitization of diamonds implanted with helium ions at temperatures from 77 to 373 K. It is established that the radiation damage decreases as the implantation temperature increases. This effect is explained by radiation-…
An analytic formulation dedicated to the design of high-frequency power transformers is presented. This approach is based on the area product, and homothetic core shapes are considered. The temperature increase of the transformer is one of the main input data. Winding losses including the effect of eddy currents are c…
We study the spatiotemporal dynamics of spatially extended nonlinear cavities containing a left-handed material. Such materials, which have a negative index of refraction, have been experimentally demonstrated recently, and allow for novel electromagnetic behavior. We show that the insertion of a left-handed material…
Palladium catalysts based on Siralox and AS aluminosilicate supports for the deep oxidation of methane were studied. With the use of XRD analysis, it was found that they were heterophase systems consisting of an amorphous aluminosilicate and γ-Al2O3 stabilized against agglomeration. It was found that the catalytic act…
Electrospun nanofiber surfaces are modified with proteins to control protein release. A mixture of poly(ε-caprolactone) (PCL) and PCL—PEG block copolymers is electrospun to prepare amine-terminated block copolymers. The amount of surface exposed amine groups increases as the blend ratio of block copolymer increases. C…
Hydrides of LaFe11.57Si1.43 intermetallic compound have been prepared by high-energy ball milling in the presence of hydrogen gas, a process known as reactive milling. The Curie temperature of the samples was tuned within the temperature range of 199 K to 346 K by changing the hydrogen content from 0 to 2.3 at. % with…
The corrosion performance of a mild steel (MS) exposed to a 0.5 M HCl solution with various concentrations of Rhodanine (Rh) was studied by means of anodic and cathodic voltammetric curves, electrochemical impedance spectroscopy (EIS) and linear polarization resistance (LPR) techniques. Rh makes the corrosion of MS in…
Abstract High-resolution synchrotron X-ray diffraction recorded on a collection of palygorskites with different chemical compositions (obtained by analytical electron microscopy) permits unambiguous correlation of the crystallographic parameters a (or a sin β if a monoclinic phase is considered) with the nature of the…
Pyridoxal kinase catalyzes the transfer of a phosphate group from ATP to the 5' alcohol of pyridoxine, pyridoxamine, and pyridoxal. In this work, kinetic studies were conducted to examine monovalent cation dependence of human pyridoxal kinase kinetic parameters. The results show that hPLK affinity for ATP and PL is in…