Materials Literature
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The challenge to develop high piezoelectric sensitivity and lead-free composition ferro-piezoelectric ceramics has recently dragged new attention to some classic ferroelectrics. Here, Ba(CexTi1-x)O3 (Ce-BT) and 0.94(Bi1/2Na1/2)TiO3-0.06BaTiO3 (BNBT6) ceramics were piezoelectrically characterized from measurements of c…
A convenient and effective 'ultrasonic dispersion method' was used to fabricate vector/DNA complexes encapsulated microspheres. Polyamidoamine (PAMAM) dendrimer/DNA complexes protected by a water-soluble polymer, poly-alpha,beta-[N-(2-hydroxyethyl)-L-aspartamide] (PHEA), were encapsulated in a polymer film mainly comp…
The main problem associated with metal hexacyanoferrates (MHCFs) is their instability at high pH values. We synthesized a new Prussian Blue analogue, Nile-Blue hexacyanoferrate (NBHCF), that remains stable in 0.2 M KOH. A carbon paste (CPE) chemically modified electrode (ME) containing NBHCF was prepared as a stable e…
The influence of the deformation of the tetrapyrrole aromatic macrocycle and the electronic effects of substituents on the kinetic parameters in the formation and dissociation reactions of cobalt complexes of porphyrins are discussed on the basis of a study of the kinetics of the formation and dissociation of cobalt c…
The paper refers to numerical modelling of the hardening process of steel C45. In the algorithm the heat transfer equation, equilibrium equations and macroscopic model of phase transformations, basis of CCT diagrams, are used. Coupling between basic phenomena of hardening process is considered, in particular the influ…
This article describes the preparation and characterization of anticancer drug-loaded poly(lactide-co-glycolide) (PLGA) microparticles. PLGA microparticles loaded with doxorubicin HCl (DOX) were prepared via o/w emulsion solvent evaporation. The release characteristics, encapsulation efficiency, size, and morphology o…
This letter reports the first demonstration of a monolithic heterostructure with a large electric tuning of the ferromagnetic resonance (FMR) at millimeter-wave frequencies. The structure is composed of a barium-strontium-titanate (BST) film and two thin platinum electrodes, all grown on a barium ferrite slab with in-…
A triple layered nanocomposite consisting of a hydrogenated layer on the surface of a core/shelled carbon nanotube/tetrahedral amorphous carbon structure was studied. The threshold field for electron emission was lowered from 4.45 to and even lower to as each layer was added. Derived from the Fowler–Nordheim plots, th…
This paper derives an exact analytical solution for determining elastic critical buckling pressures and mode shapes for very long corroded cylindrical steel shells subjected to external pressure considering symmetrical and anti-symmetrical mode cases. The corroded long cylindrical shell has been modelled as a non-unif…
AbstrAct Purpose: The objective of this work present the characterization of microstructure and properties of consolidated powder AgSn7.5Bi0.5 by using composition of cyclic extrusion compression (CEC) and hydrostatic extrusion (HE) methods. As the final product the wires of 3 mm in diameter were obtained. The compari…
Three new oxo-centered trinuclear complexes, one of them a mixed-valence complex [Mn3O(C7H4O2Cl)6(Py)3]Py (1) and the others, mixed-metal complexes of [Fe2MnO(C7H4O2Cl)6(Py)3]NO3 (2) and [Fe2CoO(C7H4O2Cl)6(Py)3] (3) were synthesized by the direct reaction between metal nitrates and p-chlorobenzoic acid. These complexe…
Zn-1.5wt.%Cu peritectic alloy was prepared in a graphite crucible under a vacuum atmosphere. Unidirectional solidification of Zn-1.5wt.%Cu peritectic alloy was carried out with the Bridgman method by using metals of 99.99 % purity under the argon atmosphere and two different conditions; with a temperature gradient (G)…
The direct application of phosphate rock seems to offer a better alternative in terms of low cost, least energy-intensive and sophistication of processing of the phosphate ore to produce soluble fertilizers. On the other hand, lower sensitivity to the ore quality offers a big advantage and the presence of impurities,…
Ultrathin carbon nanosheets (CNSs) were functionalized using 1,3 dipolar cycloaddition of azomethine ylide. The organic modification of carbon nanosheets with hydroxyl groups on the external graphene layers facilitates the dispersion in polar solvents including water and thus the incorporation of the derivatives in ot…
We have developed a new etching solution for the printed circuit board industry. The primary oxidant of the solution is nitric acid, which reacts with copper coating on the substrate. The other components of the solution are sulfuric acid and additive, which are used to control etching reaction rate and solution's cha…
TiOx, TiNy and TiOxNy thin films were deposited by reactive sputtering. The reactive gas pulsing process was implemented to tune the chemical composition and consequently, the characteristics of the films. For TiOx coatings, oxygen concentration was progressively modified from pure titanium to TiO2 compound. Similarly…
We developed a novel anti-agglomeration method that enables preservation of the vertical alignment of carbon nanotubes (CNTs) during desiccation of wet CNTs by utilizing antisolvent precipitation and sublimation of naphthalene (Nap). Moreover, we succeeded in depositing Pt nanoparticles onto CNTs without collapse of t…
In this paper, a new method to prepare particle-stabilised foams by using short chain amphiphile valeric acid was reported. Quantitative analysis of the optical microscope pictures taken at different time of particle-stabilised foams indicated that they were ultrastable and almost did not ripen and coalesce. Porous ce…
An inspiration to the research work has arisen from the problems related to cracking of massive castings made of ferritic-austenitic cast steel. The shape and the character of crack trajectories indicate that they are hot cracks. Investigations have included two cast steel grades, namely GX2CrNiMoN25-6-3 and GX2CrNiMo…
This paper reports the latest findings from studies on the role of organic matter in soil pH change. Soil pH changes induced by canola, chickpea and wheat residues in two soils with different initial pH (pH 4.4 and 6.2) were investigated under field conditions over 18 months. Changes in pH were related to ash alkalini…