Materials Literature
按标题、摘要、年份、主题和来源检索公开元数据。结果保留作者、摘要、分类与原始来源链接。
We report on the fabrication of a polypyrrole/poly(methyl methacrylate) coaxial nanocable through the sequential polymerization of methyl methacrylate and pyrrole monomers inside the channels of mesoporous SBA-15 silica, followed by the removal of the silica template.
The hydrogenation of but-2-enal over supported Au catalysts is discussed, together with a detailed characterisation study using X-ray diffraction, infrared spectroscopy and transmission electron microscopy. Au/ZnO catalysts are found to be selective for the formation of the unsaturated alcohol, but-2-en-1-ol rather th…
Low protein adsorption is believed advantageous for blood-contacting materials and ethylene glycols (EG)-based polymeric compounds are often attached to surfaces for this purpose. In the present study, the adsorption of fibrinogen, serum, and plasma were studied by ellipsometry on a series of well-defined oligo(EG) te…
Porous silk fibroin materials, with average pore size 10 ∼ 300 μm, pore density 1 ∼ 2000/mm2, and porosity 35 ∼ 70%, were prepared by freeze drying aqueous solution of silk fibroin obtained by dissolving silk fibroin in ternary solvent CaCl2 · CH3CH2OH · H2O. Pore size distribution of such materials mostly accorded wi…
Magnesium alloys are generally brittle owing to their HCP structure. In this study, improvement of tensile mechanical properties under dynamic loading has been demonstrated for a pure magnesium and a ZK60 magnesium alloy. The solution-treated ZK60 alloy exhibits yielding at a dynamic strain rate of 1.8×103 s−1, which…
The paper presents an attempt to apply spectral analysis tools in processing acoustic emission (AE) pulses generated by partial discharge (FD). The experimental part of the paper describes spark gaps generating four types of PD and specifies parameters of measured acoustic signals and recalls the system used for measu…
This 2003 book relates the complete set of strength characteristics of constituent atoms to their electronic structures. These relationships require knowledge of both the chemistry and physics of materials. The book uses both classical and quantum mechanics, since both are needed to describe these properties, and begi…
Isomorphous substitution of Fe in the MFI framework and extraction by steaming leads to a highly active and stable catalyst for N2O decomposition in tail-gas from nitric acid plants.
This study was intended to identify a high molecular weight allergen that had been detected in fish. Analyses by ELISA of five protein fractions prepared from bigeye tuna muscle showed that the high molecular weight allergen was contained in the myostromal protein fraction. Based on the results of SDS-PAGE, immunoblot…
A fully collapsed multiwalled carbon nanotube (MWCNT1) section and a different twisted and fully collapsed MWCNT were observed with tapping-mode atomic force microscopy. The collapsed section of MWCNT1 was significantly more flexible than the uncollapsed sections, and advanced 120 nm within 1 month. The collapse of MW…
A new concept of hybrid supercapacitors has been designed with a conductive polymer as the positive electrode and activated carbon as the negative electrode. The chosen polymer was poly(4-fluorophenyl-3-thiophene) or P-4-FPT, whose good doping properties are well known. Several activated carbons were tested, and the r…
The tensile properties at room temperature ∼ 573 K of Mg–9Al–1Zn processed by normal extrusion were compared with those processed by equal channel angular (ECA) extrusion. The strength at room temperature was strongly affected by the grain size. However, the effect of the grain size rapidly decreased with testing temp…
Amorphous silicon oxide thin films were prepared by the coevaporation technique in ultrahigh vacuum. Different compositions were obtained by changing the evaporation rate of silicon. The samples were then annealed to different temperatures up to 950 °C. The composition and the structure were investigated using energy…
Hollow clay microspheres of high thermal stability were easily fabricated by the adsorption of colloidal clay layers onto the surfaces of a spherical anion exchange resin and calcination of the resulting resin–clay composite.
A novel synthesis of the title compound, C2S3N3 (1) is reported. X- and K-band EPR spectra on dilute solutions of 1 indicate delocalisation of the unpaired spin density over both heterocyclic rings in agreement with DFT calculations. An XRPD study indicates that it crystallises in two morphologies with both phases for…
The current state of investigations of the problem of providing first mirrors (FMs) for diagnostic systems in a reactor-grade fusion device is summarized. Results obtained in simulation experiments that have been conducted during recent years in several laboratories are presented. Attention is concentrated on two proc…
An algorithm for the determination of the space-group symmetry of a crystal from powder diffraction data, based upon probability theory, is described. Specifically, the relative probabilities of different extinction symbols are assessed within a particular crystal system. In general, only a small number of extinction…
Abstract Solutions of both basic and acidic dyes were subject to sonolysis, electrolysis, and sonoelectrolysis. Only basic dyes were decolorized by ultrasound alone. Removal of the acidic dye Sandolan Yellow required the use of an electrooxidation process. The rate of electrochemical decolorization in the absence of u…
The preparation of nanoscale MS particles (M = Zn, Cd, Hg) with the polyol method is described. Starting with metal acetates and thiourea as precursors, by heating at 180 °C in diethylene glycol, crystalline particles 30–250 nm in size can be yielded. The resulting particle size is examined in DEG–H2O suspension apply…
Studies of pressure induced phase transformations of ZnS nanoparticles using diamond anvil cells and synchrotron radiation were carried out to 20.0 GPa. Nanoparticles initially in the zinc-blende and wurtzite phases both transformed to the NaCl phase under the application of pressure. The zinc-blende particles, which…