Materials Literature
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Direct implantation of Fe, Ni or Mn at doses of 3–5×1016 cm−2 into p-type 6H-SiC substrates was carried out at a sample temperature of ∼350 °C. Subsequent annealing was performed at 700–1000 °C for 5 mins. Residual damage in the form of end-of-range defects and dislocation loops in the region from the surface to a dep…
A white calcium bentonite (CaB) from the K\\"{u}tahya region/Turkey was activated by heating it for 6 hours at 97°C in H2SO4 solution. The mass percentage of H2SO4 in the bentonite-acid mixture was varied from 0 to 70%. The chemical analysis (CA), cation exchange capacity (CEC), differential thermal analy…
Barium strontium titanate (Ba0.8Sr0.2TiO3) thin films have been prepared on Pt/Ti/SiO2/Si substrates using a soft solution processing. X-ray diffraction and also micro-Raman spectroscopy showed that the Ba0.8Sr0.2TiO3 thin films exhibited a tetragonal structure at room temperature. The presence of Raman active modes w…
Poly(3-hydroxybutyrate) (PHB) is sensitive to high processing temperatures. This leads to a decrease in molar mass as well as a lower melt viscosity. The crystallization temperature shifts to lower values, and crystallization kinetics is slow. A mixture was developed in order to improve the manufacturing properties an…
Serine hydroxymethyltransferase (SHMT), a member of the alpha-class of pyridoxal phosphate-dependent enzymes, catalyzes the reversible conversion of serine to glycine and tetrahydrofolate to 5,10-methylene tetrahydrofolate. We present here the crystal structures of the native enzyme and its complexes with serine, glyc…
The effects of Fe oxidation state on the infrared (IR) spectra of dioctahedral smectite were studied using a purified and Na + -saturated fraction of the Garfield nontronite reference clay. The nontronite was first reduced with sodium dithionite for a period of 10 to 240 min to obtain various Fe reduction levels. The…
ABSTRACT Pea‐protein isolate solutions were heat‐denatured and dried to form stand‐alone edible films. Heat treatment at 90 °C over 5 min increased tensile strength and elongation‐at‐break, and decreased the elastic modulus. No significant differences were found in the initial contact angle of water and surface energi…
The corrosion inhibition of mild steel by some new synthesized triazole organic-type compounds, the 3,5-di(n-tolyl)-4-amino-1,2,4-triazoles (n-DTAT: n = 2, 3, 4), was investigated in 1 M hydrochloric acid (HCl) and 0.5 M sulfuric acid (H2SO4) using weight loss measurements, electrochemical impedance spectroscopy, and…
The method of invariant embedding has been applied to calculations of gamma-ray buildup factors for point isotropic sources in infinite homogeneous media up to depths of 100 mean free paths (mfp) without bremsstrahlung. A comprehensive survey of buildup factors was performed to estimate errors due to energy, angle and…
Nanocomposite materials of clay nanoparticles and polystyrene were prepared using living anionic surface-initiated polymerization (LASIP). The montmorillonite clay surface and intergallery interfaces were intercalated with 1,1-diphenylethylene (DPE), an organic cation and initiator derivative for anionic polymerizatio…
Abstract: It is clear that cross sections of wood cells show a lamellar structure. This paper investigates the orientation of this lamellar structure of spruce (Picea abies) tracheids using atomic force microscopy (AFM) and scanning electron microscopy (SEM). Cross sections of spruce wood were produced through fractur…
Partial discharge (PD) measurements have long been recognised as an important tool for detecting and predicting dielectric breakdown (BD). However, as a result of their small amplitude and wide bandwidth, the relationship between the physical mechanisms of gas breakdown and PD signal generation has not been clarified…
Adsorption of NO on Al2O3 leads to the formation of small amounts of surface nitro–nitrito (1461, 1318, 1228, 1220 and 1074 cm−1) and nitrato (1652 cm−1) complexes. Introduction of oxygen into the system causes oxidation of the NO2− compounds to nitrates (1628, 1591, 1565, 1298, 1259 and 1042 cm−1) whose concentration…
This paper describes the development of a 1.58-/spl mu/m broad-band and gain-flattened erbium-doped tellurite fiber amplifier (EDTFA). First, we compare the spectroscopic properties of various glasses including the stimulated emission cross sections of the Er/sup 3+4/ I/sub 13/2/ /sup 4/I/sub 15/2/ transition and the…
Abstract Air gaps entrapped in protective clothing are known as one of the major factors affecting heat transfer through multiple layers of flexible clothing fabrics. The identification and quantification of the air gaps are two aspects of a multidisciplinary research effort directed toward improving the flame/thermal…
An overview of the optical limiting (OL) processes in phthalocyanines and related compounds is presented, particularly a description of the synthesis and relevant optical properties of a series of axially substituted indium(III), titanium(IV), phthalo- and naphthalocyanines, and octaarylporphyrazines. Several techniqu…
The photosensitizing and pharmacokinetic properties of porphyrin-type compounds have been investigated for nearly a century. In the last decade, two porphyrin derivatives were approved in the U.S.A. and in several other countries for the photodynamic treatment of various lesions. An overview of the different mechanism…
This paper focuses on a theoretical investigation of the coupling mechanism of heat transfer and liquid moisture diffusion in porous textiles using a mathematical model developed earlier. In the model, an equation describing liquid diffusion behavior is incorporated into an energy conservation equation and mass conser…
Spectroscopic ellipsometry and atomic force microscopy (AFM) experiments are employed to characterize nanocolloidal gold films, self-assembled at APTES-derivatized Si/SiO 2 surfaces. X-ray fluorescence measurements after deposition confirm that AFM provides a representative means to probe the absolute surface coverage…
Rapid and accurate determination of the surface area of three kaolinite clay standards, taking into account the complex microtopography of the particles, was achieved using atomic force microscopy images and computerized image analysis. All surface areas were determined to within 3%. Edge surface area is 18.2-30.0% of…