Materials Literature
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Effects of pretreatment on the nuclei formation of ultrananocrystalline diamond (UNCD) on Si substrates were studied. Either precoating a thin layer of titanium (∼400nm) or ultrasonication pretreatment using diamond and titanium mixed powder (D&T process) enhances the nucleation process on Si substrates markedly,…
Polycrystalline Ba1−xSrxTiO3 (BST) thin films with three different compositions have been deposited by radio-frequency magnetron sputtering technique on platinum coated silicon substrates. Samples with buffer and barrier layers for different film thicknesses and processing temperatures have been studied. Crystallite s…
We report experiments on a ferroelectric membrane and droplets with tunable surface properties. In smectic membranes the configuration of the c -director field near inclusions may be rearranged drastically with temperature. The transformation of the c -director field results from the competition between the elastic an…
Poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) was used to fabricate micro- and nano-fibrous, non-woven mats by electrospinning for potential tissue engineering applications. The morphology and size of electrospun fibers were assessed systematically by varying the processing parameters. It was found that the diam…
We propose a phenomenological intrinsic finite-size effect model for single domain, mechanically free, and surface charge compensated PbTiO3 (PT) nanocrystals with no depolarization fields, undergoing a first-order tetragonal→cubic ferrodistortive phase transition. We then derive a Landau-Devonshire type free-energy f…
Sn 1 − x Mn x O 2 nanocrystalline powders were synthesized by a wet chemical method (x⩽0.08). X-ray diffraction reveals that single-phase rutile Sn1−xMnxO2 was obtained for x up to about 0.06. Evolution of cell parameters, x-ray photoelectron spectroscopy measurements, thermogravimetric analysis, and quantitative eval…
This work reports the influence of oxidation on the superplasticity of commercially pure titanium at high temperatures. Uniaxial tensile tests were conducted at temperatures in the range 600-800°C with an initial strain rate of 10s-1 to 10s-3. This study shows that oxidization at the surface of the alloy causes oxide…
The required complex of properties of modern pipe steels, including improved weldability and cold resistance, can be achieved due to formation of fine-grained ferrite-bainite microstructure of steel. Effect of various designs of additional alloying of steel on phase transformations with use of deformation CCT diagrams…
Authors have reported theses concerning the cast defect for publication in journal of Japanese Foundry Engineering Society and AFS Transactions. This is a review of these reports. There are various factors in the casting defect that occurs in the article of casting metal, and specific of the generation factor is diffi…
Many steels tubes used in the Oil Industry are constantly exposed to hydrogen sulphide (H2S) which can lead to the diffusion of hydrogen into the steel, potentially provoking hydrogen embrittlement and/or stress corrosion cracking. Additionally the critical region in pipelines is usually considered to be the welded jo…
Alloys based on FePd in the vicinity of the equiatomic composition are good model systems to study the microstructrual and phase transformation behavior of the class of technologically interesting ferromagnetic L10-intermetallics that includes also FePt and CoPt. Here, thermo-mechanical processing, involving cold-work…
Three main hypotheses of hydrogen embrittlement (HE) of austenitic steels are discussed based on the studies of the interatomic interactions, hydrogen-induced phase transformations and dislocations properties. Measurements of electron spin resonance and ab initio calculations of the electron structure witness that the…
Up to now, Solid Oxide Fuel Cell (SOFC) materials and processing does not meet the cost goals for commercialization. This resulted in a worldwide increase in R&D activities dealing with advanced materials and effective manufacturing methods. The present paper describes efforts to process novel SOFC materials as we…
Effect of isothermal aging on martensitic transformation temperatures, mechanical properties and microstructure was investigated for a Ni-rich Ti-Zr-Ni shape memory alloy at temperatures ranging from 673 K to 773 K. The aging behaviour was two stage process: the first stage associated with an increase in the Vickers h…
Literature data on (self-)diffusion in transition metal borides are extremely sparse due to the low atomic mobility of the constituents and due to the fact that for B there exist no suitable radioactive tracers and only two stable isotopes with a high natural abundance of 19 % (10B) and 81 % (11B), respectively. The p…
To make an expansion of composite consumption ever widening with use at demanding and safety critical applications, it is important to establish the evaluation technique of the strength, the safety, etc. To reach the goal with a useful reliable technique, we have developed a numerical simulation program on damage deve…
The physical origin of the residual stresses developed in the ceramic layer of the active region in a multilayer ceramic capacitor was numerically investigated. The compressive in-plane stress components σ11 and σ22 originate without regard to the presence of the margins but rather from the difference in in-plane ther…
Two topics are described for structure analyses of glass and liquid using a combination of conical nozzle levitation (CNL) technique and diffraction experiments. The structure of high-purity bulk forsterite (Mg2SiO4) glass synthesized by a CNL technique has been determined by a combination of high-energy x-ray, neutro…
A full 3D finite element method has been used to understand how nano-clay particles affect the mechanical properties of an epoxy/clay nanocomposite. The epoxy/clay nanocomposite has been modelled as a representative volume element (RVE) containing intercalated clay platelets that internally delaminates at the gallery…
Crystallographic macrotexture of pure niobium cold rolled to 30, 60, 80 and 90% reduction was analyzed by X-ray diffraction and compared with low carbon steel texture. Annealed samples from 800oC, to 1200oC were investigated by X-ray diffraction and electron back scattering diffraction (EBSD). The texture of cold roll…