Materials Literature
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Frequency response analysis (FRA) is an emerging, powerful non-intrusive condition monitoring and diagnostic tool for verifying the mechanical integrity of power transformers. FRA results are graphical in nature and require trained experts to interpret test results. The work reported discusses numerical-criteria-based…
Blue light-emitting anthracene derivatives end-capped with triphenylamine for efficient hole transportation have been designed and synthesized using two-step Suzuki coupling reactions. The compounds possess high glass transition temperatures for good thermal stability and strong blue emission in solution. Typical thre…
Six new lead coordination polymers, namely, [Pb(INO) 2 ]·3H 2 O ( 1 ), [Pb(INO) 2 ·NO 3 ·H 2 O] ( 2 ), [Pb(INO)·Cl] ( 3 ), Na 1.5 [Pb 2 (INO) 5 ]·0.5NO 3 ( 4 ), [Pb 3 (NNO) 4 ·(NO 3 ) 2 ·H 2 O] ( 5 ), and [Pb(NNO) 2 ] ( 6 ), have been prepared by the reaction of Pb(NO 3 ) 2 with isonicotinic acid N-oxide (HINO), or ni…
Lithographically patterned nanowire electrodeposition (LPNE) is a new method for fabricating polycrystalline metal nanowires using electrodeposition. In LPNE, a sacrificial metal (M(1)=silver or nickel) layer, 5-100 nm in thickness, is first vapor deposited onto a glass, oxidized silicon, or Kapton polymer film. A (+)…
Rare hysteretic adsorption/desorption isotherms are reported for CO2 and N2 on a pillared Ni(1,2-bis(4-pyridyl)ethylene)[Ni(CN)4] compound (NiBpeneNiCN). The hysteresis occurs under moderate pressure and at temperatures above the critical temperatures of the respective gases. Powder X-ray diffraction measurements indi…
Melamine, a nitrogen-rich chemical, was implicated in pet and human food recalls in 2007, which caused enormous economic losses to the food industry. In this study, melamine concentration in wheat gluten, chicken feed, and processed foods (that is, cake and noodle) was measured by surface enhanced Raman spectroscopy (…
The effect of surface inorganic−organic interactions on magnetic and structural properties of iron oxide magnetic nanoparticles functionalized by lipophilic stilbene molecules has been investigated. The molecules have been grafted through either phosphonate or carboxylate coupling agents. Mössbauer spectra recorded at…
Strong magnetic fluctuations can provide a coupling mechanism for electrons that leads to unconventional superconductivity. Magnetic order and superconductivity have been found to coexist in a number of magnetically mediated superconductors, but these order parameters generally compete. We report that close to the upp…
First principles density functional theoretical calculations were carried out to examine and compare the reaction paths and ensembles for the electrocatalytic oxidation of methanol and formic acid in the presence of solution and applied electrochemical potential. Methanol proceeds via both direct and indirect pathways…
We experimentally demonstrate extremely narrow plasmon resonances with half-width of just several nanometers in regular arrays of metallic nanoparticles. These resonances are observed at Rayleigh's cutoff wavelengths for Wood anomalies and based on diffraction coupling of localized plasmons. We show experimentally tha…
The hydrogen evolution reaction (HER) on carbon supported MoS2 nanoparticles is investigated and compared to findings with previously published work on Au(111) supported MoS2. An investigation into MoS2 oxidation is presented and used to quantify the surface concentration of MoS2. Other metal sulfides with morphologie…
Abstract Polypropylene (PP)/metallocene‐catalyzed polyethylene elastomer (mPE) blends were prepared in a twin‐screw extruder. The melting behavior, crystallization behavior, and isothermal crystallization kinetics of the blends were studied with differential scanning calorimetry. The results showed that PP and mPE wer…
Founded in 1683 in Leiden, the Netherlands, Brill is a leading international academic publisher in the Humanities, Social Sciences, International Law, and Biology. With offices in the Netherlands, Germany, Austria, the USA and Asia, Brill today publishes more than 360 journals and 2,000 new books and reference works e…
The iron(III) compound of formula [3-pmH · 3-pm][Fe(NCS)4(3-pm)2] (3-pm = 3-(hydroxymethyl)pyridine) has been prepared by reaction between iron(III) thiocyanate and 3-(hydroxymethyl)pyridine in ethanol. The characterization was based on elemental analysis, infrared spectra and magnetic measurements. Single crystal X-r…
Brillouin light scattering has been used to investigate the density fluctuations of the fragile glass-former sorbitol in the GHz frequency range and at temperatures between 20 and 294 K. Longitudinal acoustic sound velocity and attenuation data are here reported and discussed. These data are used to test the existence…
A method has been developed for retrieving the complete angular selectivity profile of transmission holographic gratings in one step. The method is applied to study in real time the shrinkage and changes in the effective optical thickness of a slanted holographic grating recorded in an acrylamide-based photopolymer. I…
Boron-nitride nanocones with $60\ifmmode^\circ\else\textdegree\fi{}$, $120\ifmmode^\circ\else\textdegree\fi{}$, and $240\ifmmode^\circ\else\textdegree\fi{}$ disclination under the influence of parallel and perpendicular external electric fields are studied through first-principles calculations based on the density-fun…
The effects of low-temperature annealing and oxidation of the dilute magnetic semiconductor ${\text{Ga}}_{1\ensuremath{-}x}{\text{Mn}}_{x}\text{As}$ are studied by photoemission spectroscopy in the hard x-ray regime (HAXPES), with special attention to the depth profile of both concentration and chemical state of manga…
In a previous paper ( Macromolecules 2007, 40, 5923), we reported that a zone heating method, which imposes the moving temperature-gradient (∇ T ) field on ordering process of various melts in general, enabled to control a macroscopic orientation of hexagonally packed cylindrical microdomain structures (hex-cyl) of bl…
Abstract Temperature and composition dependence of the dc resistivity ( ρ dc ) and thermoelectric power ( α ) of Li 0.3–0.5 x Zn 0.4 Ca x Fe 2.3–0.5 x O 4 ferrites ( x = 0.0, 0.01, 0.02, 0.03 and 0.05), prepared by the standard ceramic method, have been studied. The behavior of both ρ dc and α with temperature support…