Materials Literature
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The aligned CdS nanorods are obtained by dispersing CdS in the conducting polyaniline matrix. The rods are about 50 nm in diameter and 400 nm in length. The significant changes of electronic absorption spectra of CdS nanorods and conducting polyaniline indicate the strong interaction between them. CdS—Polyaniline nano…
The characterization of technetium (Tc) environments in borosilicate glasses is important with regard to the long-term isolation of Tc in nuclear wastes from the environment by waste vitrification. In this study, Raman spectroscopy was used to detect Tc in various borosilicate waste glass formulations in which Tc vale…
Abstract This work aims at studying of electrochemical oxidation of porous silicon (PSi) and its behaviour in simulated body fluid (SBF). Continuing electrochemical oxidation of PSi introduces gradual changes in morphology of the porous structure and composition of PSi. As a result, interaction between this material a…
Abstract Zinc and hot dip galvanized steel are frecuently used metals in building application. They have relatively good atmospheric resistance to corrosion, due to its oxidation in air and formation of protective rust on its surface, which acts as barrier between the metal and environment. However, some part of the r…
The streaming potential generated by pressure-driven two-phase flow in a circular capillary differs from that generated by single-phase flow. Three model problems are considered, in which the dispersed phase consists of either (i) a rigid spherical particle (possibly charged), (ii) an uncharged spherical bubble, and (…
We report on electrical bias voltage manipulation of the magnetic domain structures of patterned ferromagnetic Fe dots on a ferroelectric BaTiO3 underlayer using a scanning probe microscope technique. Piezoresponse force microscopy is used to apply local electric field on the Fe dots/BaTiO3 hybrid structure and to map…
A novel force-field development strategy is proposed that tackles the well-known difficulty of parameter correlations arising in a conventional least-squares optimization. In the first step of the new gradient curves method (GCM), continuity criteria are imposed to transform the raw multidimensional ab initio training…
A new cardenolide, 3-O-(beta-glucopyranosyl)acovenosigenin A (1), was isolated from the roots of Streptocaulon griffithii, together with eight known cardenolides, compounds 2-9. All compounds showed significant in vitro inhibition of the proliferation of the human gastrointestinal cancer cell line HGC-27, with IC50 va…
The dynamic mechanical properties were obtained over a wide range of temperatures and strains on vulcanisates filled with carbon black (N330) and a modified carbon black respectively. The modified carbon black (GCB) was prepared by adding special resorcinol formaldehyde latex (RFL) into N330. The main chain of RFL has…
Ultrasonic or stirring agitation of silicon‐based pre‐ceramic polymer emulsions in water, followed by crosslinking and consecutive pyrolysis was used to produce fine disperse powders of Si/C/O ceramic particles with spherical morphology. Depending on the shear forces introduced during the formation of the emulsions th…
The first syntheses of polyyne-containing sphingoid base analogues were achieved by employing our iterative strategy that uses a two-step acetylene homologation sequence. In this process, a bromoalkyne is homologated by one acetylene unit through a Pd-catalyzed cross-coupling with a TIPS-protected acetylene and a subs…
The purpose of this study was to characterize essential changes in the structure of annulus fibrosus (AF) after hydrothermal and infrared (IR) laser treatment and to correlate these results with alterations in tissue state. Polarization-sensitive optical coherence tomography imaging was used to measure collagen birefr…
Melt intercalation of montmorillonite (MMT) into polymeric matrices to improve the mechanical properties of polymers has evolved into a subject of tremendous fundamental and technological interest. The thermal treatment experienced during processing or end use can substantially affect the clay and diminish the target…
Nanorod field-effect transistors (FETs) that use multiple Mg-doped ZnO nanorods and a SiO2gate insulator were fabricated and characterized. The use of multiple nanorods provides higher on-currents without significant degradation in threshold voltage shift and subthreshold slopes. It has been observed that the on-curre…
A highly stable, reproducible and water‐based bismuth titanate (BTO) sol system has been synthesized by an aqueous sol–gel method. First bismuth nitrate was dissolved in acetic acid, and then it was mixed with a solution of lactic acid dissolved tetra‐ n ‐butyl titanate, subsequently, water was added to adjust sol con…
The encapsulation of molecules into nanocarriers is studied for its potential in delivering a high dose of anticancer drugs to a tumor, while minimizing side effects. Most systems either release their content in a non-specific manner or under specific environmental conditions such as temperature or pH. We have synthes…
Recent studies of microdiamonds from orogenic belts related to continental collisions induced experimentalists to explore new crystallization media possible for diamond synthesis. This has led to considerable progress in diamond-synthesis experiments under high pressures and high temperatures. Diamond was found to gro…
Variations in cation occupancy in mixed metal ferrite systems can affect their electronic and magnetic properties. It is known that different synthesis parameters can lead to various cation distributions and the ability to tune these distributions is of great interest. This study uses the extended x-ray-absorption fin…
Slow strain rate tests (SSRT) were used to investigate stress corrosion cracking (SCC) behavior of an X-70 pipeline steel in a soil solution and NS-4 solution, both saturated with 5% carbon dioxide (CO2)/balance N2 gas mixture at different potentials and strain rates. It was found that transgranular SCC occurred in th…
In the present work a simple but selective reversed‐phase high performance liquid chromatographic method (HPLC) was developed for the analysis of the nematic liquid crystal mixture E7 to determine precisely the composition of the liquid crystal mixture used in PDLC film preparation. Ultraviolet absorption spectrophoto…