Materials Literature
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Highly oriented perovskite films of PbMg1/3Nb2/3–PbTiO3 and PbSc1/2Nb1/2O3–PbTiO3 with compositions near the morphotropic phase boundary were formed by pulsed laser deposition on La0.5Sr0.5CoO3/MgO (100). The dielectric properties of the films were studied over the frequency range of 100 Hz–1 MHz in the temperature ra…
A spectrum-inversion approach to extract information from MQ-MAS NMR spectra in glasses is presented. This allows the reconstruction of the underlying two-dimensional distribution of the isotropic chemical shift correlated to the quadrupolar interaction. The dependency upon the quadrupolar interaction and the RF field…
Both selenomethionine (SeMet) based multiwavelength anomalous diffraction (MAD) phasing and protein production in baculovirus expression vector systems have greatly enhanced the scope and speed of macromolecular crystallography, but the apparent incompatibility of these two powerful techniques presents an obstacle to…
Optical reflectivity spectra were measured on cleaved surfaces of ${\mathrm{La}}_{0.825}{\mathrm{Sr}}_{0.175}{\mathrm{MnO}}_{3}$ single crystals ${(T}_{\mathrm{C}}=283$ K) over a temperature range 10--295 K. The optical conductivity $\ensuremath{\sigma}(\ensuremath{\omega})$ shows incoherent-to-coherent crossover with…
The fracture behavior of an oxide/oxide ceramic‐matrix composite, alumina/alumina‐silica (Nextel610/AS), was investigated at 23° and 950°C using a single edge notched specimen geometry with clamped ends. Crack growth and damage progression were monitored during the tests using optical microscopy, ultrasonic C‐scans, a…
Stable organic biradical crystals PNNNO, ${\mathrm{F}}_{2}\mathrm{PNNNO},$ and PIMNO of the PNNNO family were synthesized. ${\mathrm{PNNNO}=2\ensuremath{-}[{4}^{\ensuremath{'}}\ensuremath{-}$ $(N\ensuremath{-}\mathit{tert}\ensuremath{-}\mathrm{butyl}\ensuremath{-}N\ensuremath{-}\mathrm{oxyamino})\mathrm{phenyl}]\ensur…
Amorphous materials in the system , with or without the addition of , were synthesized by mechanical milling treatment of starting oxides in a dry atmosphere at room temperature. These materials, obtained as fine powders, worked as an anode for a lithium‐ion secondary battery using a conventional liquid electrolyte. T…
Raman spectra were measured for the full range of hole doping of the orthomanganites of the form ${\mathrm{La}}_{1\ensuremath{-}x}{\mathrm{Ca}}_{x}{\mathrm{MnO}}_{3}$ $(0<~x<~1)$ from ambient temperature to 75 K. Two high-frequency phonons that we assign to stretching modes of the oxygen atoms in the ${\mathrm{M…
The scanning reference electrode technique (SRET) has been used to study the influence of a range of anodic and cathodic corrosion inhibitors on patterns of localized corrosion occurring on the intact zinc surface of galvanized sheet steel. SRET spatially can resolve localized anodic and cathodic activity occurring ac…
The photocurrent measurements in combination with a modulation of the depletion region is a method which has the potentiality to determine the diffusion length profile in semiconductors directly. In this article the method is applied to strongly compensated (Au-doped) silicon. The expressions for signal description ar…
The highly branched ester rac-1 has been prepared. It exists in the form of a conglomerate (m.p. 90–92 °C) in which the two enantiomers are present in separate crystal lattices, as indicated by the melting point diagram. Both enantiomers of 1 have been isolated by crystallization [m.p. 112–114 °C, [α]D22 = +24.4 ± 0.7…
The paper presents the results of a study of kinetics of the recombination processes in crystals LiB3O5 (LBO) obtained by the use of time-resolved luminescence and optical absorption spectroscopy. It was revealed that the observed peculiarities of the recombination processes in LBO are due to a participation of the tr…
Highly oriented strontium barium niobate (SBN) thin films have been grown on MgO {100}substrates by pulsed laser deposition. The films have been characterised by X-ray diffraction (XRD), scanning electron microscopy and atomic force microscopy. XRD theta - 2 theta scans indicate that the single phase crystalline SBN l…
Abstract Preliminary investigations to study the feasibility of using polystyrene grafted with acrylic acid to blend polystyrene (PS) and nylon 6,6 (N66) have been done. The graft copolymer (PS‐g‐AA) was synthesized by reacting polystyrene with acrylic acid in the presence of a free radical initiator using the solid p…
Highly oriented strontium barium niobate (SBN) thin films have been grown on MgO{100} substrates by pulsed-laser deposition. The films have been characterized by X-ray diffraction (XRD), scanning electron microscopy and atomic force microscopy. XRD θ–2θ scans indicate single-phase crystalline SBN layers with the {100}…
This paper presents a new foaming technology using supercritical carbon dioxide as a blowing agent to obtain large volume expansion of biodegradable polyester foams of over forty-fold. The basic approach for the promotion of a large volume expansion ratio with carbon dioxide was to prevent cell coalescence by using a…
Abstract Fourier Transform Raman spectroscopy is employed to study the mechanism of reversion and the influence of the antireversion agent, 1,3 bis(citraconimidomethyl)benzene (BCI-MX) in squalene as well as in low molecular weight synthetic polyisoprene. The formation of non-sulfidic main chain modifications, such as…
A lamellar ABA triblock copolymer brought to equilibrium in the presence of a B-compatible solvent generally swells or transforms into an A-dispersed (cylindrical or micellar) morphology, depending on solvent content. If the A blocks of the copolymer are glassy, they serve as physical cross-links and stabilize a gel n…
Ytterbium–yttrium mixed oxides, which are potential emitter materials for thermophotovoltaic energy converters, were prepared using two different synthesis methods. The results of a characterization using Raman spectroscopy and x-ray powder diffraction (XRD) are presented. The purpose of this study was to confirm whet…
The structural parameters of needle punched nonwoven composites have been examined using image analysis system. Fourteen plies of carded webs of E Glass fiber were stacked and needle punched at different punching densities of 15, 30, 45, 60, and 90 penetrations per square centimeter. The needle punched webs were forme…